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Doctoral Thesis
DOI
https://doi.org/10.11606/T.85.2009.tde-22092011-150206
Document
Author
Full name
Aparecido Edilson Morcelli
E-mail
Institute/School/College
Knowledge Area
Date of Defense
Published
São Paulo, 2009
Supervisor
Committee
Andrade, Arnaldo Homobono Paes de (President)
Buso, Sidnei José
Calvo, Wilson Aparecido Parejo
Kiyohara, Pedro Kunihiko
Vatavuk, Jan
Title in Portuguese
Estudo dos micromecanismos de deformação e fratura da liga de Titânio Ti-6AI-4V utilizando-se técnicas de microscopia eletrônica e difração de Raios- X
Keywords in Portuguese
ligas de titânio
mecânica da fratura
microscopia eletrônica
Abstract in Portuguese
A realização do presente trabalho permitiu o estudo dos micromecanismos de deformação e fratura da liga de titânio Ti-6Al-4V, utilizada comercialmente para a fabricação de biomateriais metálicos. As técnicas empregadas para a análise do material em estudo foram: microscopia eletrônica de varredura (MEV), microscopia eletrônica de transmissão (MET) e a difração de raios X (DRX). Estudar a influência e comportamento das diversas fases existentes em ligas de titânio é importante para se avaliar o comportamento de trincas nas ligas de titânio com alta resistência mecânica, que possuem microestrutura fina, relacionando a presença das fases alfa (α), beta (β) e alfa+beta (α+β) com a resistência do material. A avaliação in situ dos micromecanismos de deformação e fratura foi realizada por MET e também foi feito o estudo das transformações de fase durante o resfriamento em ligas de titânio, por MET, utilizando-se as técnicas de campo claro, campo escuro e difração de elétrons (DEAS), em área selecionada. Após tratamento térmico foram observadas as diferenças entre a quantidade das fases α e β, em relação à microestrutura original do material para diferentes condições utilizadas no tratamento térmico aplicado à liga metálica. Observou-se a presença da microestrutura lamelar, formada durante o resfriamento no campo β, promovendo a transformação de parte da estrutura alfa secundária em beta, que se encontrava retida entre as lamelas de alfa.
Title in English
Study of deformation and fracture micromechanisms of titanium alloy Ti-6Al-4V using electron microscopy and X-ray difraction techniques
Keywords in English
electron microscopy
titanium alloy
Abstract in English
This present work allowed the study of deformation and fracture micromechanisms of titanium alloy Ti-6Al-4V, used commercially for the manufacture of metallic biomaterials. The techniques employed for the analysis of the material under study were: scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The study of the influence and behavior of the phases present in titanium alloys is important to evaluate the behavior of cracks in titanium alloys with high mechanical strength, which have fine alpha (α), beta (β) and alpha+beta (α+β) microstructure, linking the presence of the phases with the strength of the material. The evaluation in situ of deformation and fracture micromechanisms were performed by TEM and was also a study of phase transformations during cooling in titanium alloys, using the techniques of bright field, dark field and diffraction of electrons in the selected area. After heat treatment differences were observed between the amount of in relation to the original microstructure of the β and α phases material for different conditions used in heat treatment applied to the alloy. The presence of lamellar microstructure formed during cooling in the β field was observed, promoting the conversion of part of the secondary alpha structure in β phase, which was trapped between the lamellar of alpha.
 
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Publishing Date
2011-10-17
 
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