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Master's Dissertation
DOI
https://doi.org/10.11606/D.97.2009.tde-24102012-130437
Document
Author
Full name
Renato Baldan
Institute/School/College
Knowledge Area
Date of Defense
Published
Lorena, 2009
Supervisor
Committee
Nunes, Carlos Angelo (President)
Barboza, Miguel Justino Ribeiro
Rosenthal, Ruben
Title in Portuguese
Processamento e caracterização de rotores automotivos da superliga MAR-M247
Keywords in Portuguese
Fundição por cera perdida
MAR-M247
Superligas de níquel
Thermocalc
Tratamento térmico MAR-M247
Abstract in Portuguese
A superliga policristalina à base de níquel MAR-M247 foi desenvolvida na década de 70. Sua ótima composição, estabilidade microestrutural, excelente resistência à fluência e à oxidação e boa resistência à corrosão a quente faz dessa superliga uma das mais utilizadas em rotores durante os últimos 20 anos. Os objetivos do presente trabalho são a produção e caracterização microestrutural e mecânica de rotores da superliga MARM247 (10% peso Co, 10W, 8.25Cr, 5.5Al, 3Ta, 1.5Hf, 1Ti, 0.7Mo, 0.15C, 0.05Zr, 0.015B, Ni balanço). Os rotores foram obtidos pela técnica de microfusão por cera perdida na empresa Açotécnica S.A. (Jandira/SP) em diferentes temperaturas de vazamento e isolamento do molde cerâmico. Os materiais foram analisados por microscopia ótica e eletrônica de varredura (MEV/EDS), análise térmica diferencial (DTA), macro/microdureza e ensaios de tração convencional a 25oC e a 760oC. Além disso, os materiais passaram por tratamentos térmicos de solubilização e envelhecimento em diferentes temperaturas e tempos a fim de avaliar as mudanças microestruturais. Com a ajuda do software de cálculo termodinâmico Thermocalc foram feitas simulações das relações de fases utilizando a composição média da superliga MAR-M247. Os resultados permitiram obter uma condição de processamento (temperatura de vazamento e condição de isolamento) com maior quantidade de peças sem defeitos. Além disso, os experimentos permitiram definir uma condição ideal para o tratamento térmico de solubilização da superliga MAR-M247.
Title in English
Processing and characterization of nickel based superalloy MARM247 turbine wheels
Keywords in English
Investment casting
MAR-M247
MAR-M247 heat treatment
nickel based superalloys
Thermocalc
Abstract in English
The polycrystalline nickel-based superalloy MAR-M247 was developed in the 1970s. Its optimal alloy composition, microstructural stability, excellent resistance to creep and oxidation and good resistance to hot corrosion make the MAR-M247 superalloy one of the alloys widely used in turbine rotors during the last 20 years. The aims of the present work are the production and the microstructural and mechanical characterization of rotors made of MAR-M247 superalloy (10 wt. % Co, 10W, 8.25Cr, 5.5Al, 3Ta, 1.5Hf, 1Ti, 0.7Mo, 0.15C, 0.05Zr, 0.015B, Ni balance). The rotors were produced by using the lost-wax technique at different pouring temperatures and isolation of the shell mold at the Açotécnica S.A. company (Jandira/SP). The materials were analyzed by optical and scanning electron microscopy (SEM/EDS), differential thermal analysis (DTA), macro/microhardness and tensile tests at 25oC and 760oC. Besides, the materials were submitted to solution and ageing treatments at different temperatures and times in order to evaluate de microstructural changes. With the aid of the thermodynamic calculation software Thermocalc, simulations of phase relations were made using the average composition of the MAR-M247 superalloy. The results allowed to obtain a processing condition (pouring temperature and isolation condition) with larger amount of rotors without defects. Moreover, the experiments allowed to define an ideal solution heat treatment condition of MAR-M247 superalloy.
 
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Publishing Date
2012-10-24
 
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