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Doctoral Thesis
DOI
https://doi.org/10.11606/T.87.2008.tde-21012009-115422
Document
Author
Full name
Miriam Lúcia Chiquetto Machado
Institute/School/College
Knowledge Area
Date of Defense
Published
São Paulo, 2008
Supervisor
Committee
Pradella, Jose Geraldo da Cruz (President)
Bonomi, Antonio Maria Francisco Luiz José
Gouvêa, Míriam Tvrzská de
Hokka, Carlos Osamu
Kilikian, Beatriz Vahan
Title in Portuguese
Estudos das propriedades mecânicas e térmicas do polímero biodegradável poli-3-hidroxibutirato (PHB) e de compósitos PHB/pó de madeira.
Keywords in Portuguese
Irradiação de materiais
Poli-3-hidroxibutirato
Processamento de materiais
Propriedades mecânicas
Propriedades térmicas
Abstract in Portuguese
O objetivo deste trabalho foi o estudo das propriedades mecânicas e térmicas do PHB e de compósitos de PHB/pó de madeira processados, reprocessados e irradiados. Foram preparados compósitos com PHB e pó de madeira com concentrações de PHB/pó de madeira de 90/10, 80/20 e 70/30 (m/m). Foram realizados ensaios de propriedades mecânicas, HDT, ponto de amolecimento Vicat, TGA e DSC. A incorporação do pó de madeira aumentou o grau de cristalinidade e a temperatura de cristalização do polímero, e nos compósitos PHB/pó de madeira 80/20 e 70/30 a rigidez do material aumentou em relação ao polímero puro. O compósito PHB/pó de madeira 70/30 apresentou os melhores resultados em termos econômicos, de processamento e de estabilidade em relação ao reprocessamento. A irradiação após o processamento, em dose de 30 kGy, provocou aumento da rigidez do PHB puro e dos compósitos PHB/pó de madeira 90/10 e 80/20, embora as outras propriedades tenham decrescido. O compósito PHB/pó de madeira 70/30 apresentou queda de todas as propriedades com a irradiação.
Title in English
Study of mechanical and thermal properties of the biodegradable polymer poly-3-hydroxybutyrate (PHB) and PHB/wood flour composites.
Keywords in English
Materials irradiation
Materials processing
Mechanical properties
Poly-3-hydroxybutyrate
Thermal properties
Abstract in English
The purpose of this work was the study of the mechanical and thermal properties of processed, reprocessed and irradiated PHB, as well as PHB/wood flour composites. PHB/wood flour composites were prepared with PHB/wood relation of 90/10, 80/20 e 70/30 (w/w). Mechanical properties, HDT, Vicat melting point and thermo analyses (TGA and DSC) tests were carried out. The introduction of the wood flour increased both polymer crystallinity and crystallization temperature. The material stiffness increased in PHB/wood flour composites (80/20 and 70/30) resulting in higher values in some properties when compared with pure PHB. The PHB/wood flour composite 70/30 showed the best results in terms of economy, processing and stability during reprocessing. The irradiation after processing in 30kGy doses led to a stiffness increasing of pure PHB and PHB/wood flour composites (90/10 and 80/20) while other properties have decreased. The PHB/wood flour 70/30 showed decreasing in all properties after irradiation.
 
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Publishing Date
2009-03-19
 
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