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Master's Dissertation
DOI
https://doi.org/10.11606/D.59.2002.tde-26012007-213607
Document
Author
Full name
Adevailton Bernardo dos Santos
Institute/School/College
Knowledge Area
Date of Defense
Published
Ribeirão Preto, 2002
Supervisor
Committee
Baffa Filho, Oswaldo (President)
Pela, Carlos Alberto
Rossi, Alexandre Malta
Title in Portuguese
Estudo preliminar de RPE em banda K de esmalte dental e hidroxiapatita sintética irradiados
Keywords in Portuguese
Banda-K
Dosimetria
Esmalte Dental
Hidroxiapatita
Ressonância Paramagnética Eletrônica (RPE)
Abstract in Portuguese
A hidroxiapatita e o esmalte dental são, na atualidade, alguns dos materiais mais pesquisados pela técnica de espectroscopia por Ressonância Paramagnética Eletrônica ? RPE. O esmalte dental, que possui cerca de 97% de sua massa constituída por cristais de hidroxiapatita, se apresenta como o tecido humano preferencial para dosimetria de radiação com o uso desta técnica, principalmente no caso de exposições acidentais da população em geral. A análise de hidroxiapatitas sintéticas tem por finalidade auxiliar o entendimento do espectro do esmalte dental bem como desenvolver um dosímetro de radiação com boa eficiência e eficácia. O espectrômetro em banda-K utiliza uma freqüência intermediária aos espectrômetros em banda-X e em banda-Q, possuindo uma melhor resolução que banda-X sem as dificuldades, devido à alta sensibilidade, do banda-Q. O presente trabalho tem como objetivo analisar espectros em banda-K de um bloco de esmalte irradiado e de hidroxiapatitas sintéticas, comparando com espectros de banda-Q e banda-X presentes na literatura, e ainda verificar a possibilidade de se fazer dosimetria de radiação com o uso deste aparelho.
Title in English
Preliminary Study of EPR in K-Band of Dental Enamel and Hydroxyapatite Synthetic Irradiated.
Keywords in English
Dosimetry
Electron Paramagnetic Resonance (EPR)
Hydroxyapatite
K-Band
Tooth Enamel
Abstract in English
Hydroxyapatite and tooth enamel are, nowadays, some of materials mostly investigated by the spectroscopic technique of Electron Paramagnetic Resonance ? EPR. Tooth enamel, that have about of 97% of its mass constituted by hydroxyapatite crystals, appears itself as the preferential human tissue for radiation dosimetry using EPR, mainly in case of accidental expositions by ordinary personnel. The analyses of synthetic hydroxyapatites have as the main goal to help the understanding of tooth enamel?s spectrum seeking the developing of a radiation dosimeter with good efficiency and accuracy. The K-band EPR spectrometer uses an intermediate frequency between the spectrometers in X-band and Q-band, possessing a better resolution than the X-band without presenting the Q-band?s difficulties. In this preliminary work the EPR spectra of a small block tooth enamel and synthetic hydroxyapatites irradiated were analyzed in K-band, comparing the results with X- and Q-band with published results, the possibility of performing radiation dosimetry at K-band was verified.
 
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disserta__o.pdf (1.18 Mbytes)
Publishing Date
2007-03-02
 
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