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Master's Dissertation
DOI
https://doi.org/10.11606/D.3.2009.tde-22102009-180225
Document
Author
Full name
Paulo Henrique Ogata
E-mail
Institute/School/College
Knowledge Area
Date of Defense
Published
São Paulo, 2009
Supervisor
Committee
Goldenstein, Hélio (President)
Bott, Ivani de Souza
Gorni, Antonio Augusto
Title in Portuguese
Caracterização microestrutural do aço para tubo API 5L-X65 em diferentes regiões da chapa como laminada e após austenitização e resfriamento sob diversas taxas de resfriamento.
Keywords in Portuguese
Ensaios da estrutura dos materiais
Ensaios não destrutivos
Materiais ferrosos
Microscópio eletrônico
Microscópio ótico
Revenido
Solubilização
Trabalho em metal
Abstract in Portuguese
Este trabalho tem por objetivo caracterizar e comparar as microestruturas de diferentes regiões de uma chapa de aço microligado para tubo API 5L X65, empregado no transporte de gás natural e petróleo, como recebido e submetido a tratamentos térmicos de austenitização e resfriamento contínuo sob diferentes taxas de resfriamento. O aço em estudo apresenta uma linha de segregação central, originada durante o processo de produção do aço. Corpos de prova de dilatometria foram usinados da região central e de outras regiões da chapa. As amostras foram previamente austenitizadas a 1200°C e temperadas em água, visando solubilizar grande parte dos precipitados presentes no aço. Após este tratamento, as amostras foram austenitizadas em um dilatômetro de têmpera a 950°C por 180s, e em seguida resfriadas nas seguintes taxas de resfriamento: 0,5°C/s, 1°C/s, 5°C/s, 10°C/s, 20°C/s, 30°C/s, 40°C/s, 50ºC/s e 60ºC/s. Valores de temperatura e tempo correspondentes a inflexões da curva dilatométrica foram obtidas e correlacionadas com a microestrutura, para cada taxa de resfriamento. Com base nesta análise foi traçado um diagrama de Transformação por Resfriamento Contínuo (TRC) do material.
Title in English
Microstructural characterization of a plate of microalloyed pipeline steel that conforms to API 5L X65 in different regions of the plate as rolled and after austenitization and continous cooling under different cooling rates.
Keywords in English
Ageing treatment
CCT diagram
High strength low alloy steel
Microstructure
Segregation
Abstract in English
This work aims to characterize and compare the microstructures of different regions of a plate of microalloyed pipeline steel that conforms to API 5L X65, employed in the transportation of natural gas and oil, as received and after being subjected to heat treatments of austenitization and continuous cooling under different cooling rates. The steel under study presents a central line of segregation that was originated during production. Specimens for dilatometry were machined from the central region and from different regions of the plate. The samples were austenitized at 1200°C and in quenched in water, with the purpose of solubilizing most of the precipitates in the steel. After the preliminary heat treatment, the specimens were austenitized at 950°C for 180s and cooled under the cooling rates: 0.5°C/s, 1°C/s, 5°C/s, 10°C/s, 20°C/s, 30°C/s, 40°C/s, 50ºC/s and 60ºC/s in a quench dilatometer. Values of temperature and time correspond of transformation for each rate of cooling were used for the determination of the Continuous Cooling Transformation (CCT) diagram.
 
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Publishing Date
2010-01-07
 
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